Niget: NanoIndentation General Evaluation Tool

7 Tangent method

The method is based on the linear model as described in [3]. It is recommended only for use with highly plastic materials where the depth of elastic recovery is less than 10 % of max.

Figure 7: Tangent method analysis

7.1 Window

The window consists of several blocks:

  • Info displays the maximum depth and force during the indentation

  • Parameters shows the selected range in nm and in % of the maximum force, and the correction \beta.

    • -

      The fitting range can be selected either using the mouse or typing in the range entries. The range can be defined either in nm or in percent of the maximum force. It is often recommended to use the range 70–95 % F{}_{\mathrm{max}} for the fit, see section 7.2.

    • -

      The parameter \beta accounts for any deviations from the axisymmetric case and is used in the calculation of the reduced modulus in equation (10). Currently, the default value is the value for three-sided pyramides \beta=1.034. The value supplied by the user is saved in the settings and can be reset to its default value.

  • Fit button, see section 7.2 for details of the calculation.

  • Results displays all results in the following order: the contact depth h_{\mathrm{c}}, the slope S, the contact area A_{\mathrm{p}}(h_{\mathrm{c}}), the indentation hardness H_{IT}, the contact modulus E_{r}, the indentation modulus E_{IT} and the ranges used for the fitting procedure. The variables are described in detail in section 7.2.

  • Save save parameters and results to given file.

  • Graph display the unloading curve and the fitted curves. Stepwise zooming/unzooming can be performed by selecting a range with the mouse and pressing the Zoom/ Unzoom buttons. The graph is restored to its original size by the Restore button.

7.2 Procedure

The tangent method uses a different approach to determine the slope of the unloading curve at its maximum depth than the Oliver Pharr method.

  1. 1.

    Fit the uppermost part of the unloading curve with a straight line using a Deming fit with \delta=\sigma_{F}^{2}/\sigma_{h}^{2}, see section A.2,


    using total least squares. The range should be approx. 70–95 % F{}_{\mathrm{max}}.

  2. 2.

    Set \varepsilon=0.75 and calculate the contact depth as

    h_{\mathrm{c}}=h_{\mathrm{max}}-\varepsilon F_{\mathrm{max}}/S. (16)
  3. 3.

    Same as step 4 in 5.2.