Niget: NanoIndentation General Evaluation Tool

5 Oliver Pharr

For a definition of the Oliver Pharr method see [11].

Figure 5: Oliver-Pharr analysis

5.1 Window

The window consists of several blocks:

  • Info displays the maximum depth and force during the indentation

  • Parameters shows the selected range in nm and in % of the maximum force, and the correction \beta.

    • -

      The fitting range can be selected either using the mouse or typing in the range entries. The range can be defined either in nm or in percent of the maximum force. It is often recommended to use the range 0.5–15 % F{}_{\mathrm{max}} for the hp fit and 40–98 % F{}_{\mathrm{max}} for the S fit, see section 5.2.

    • -

      The parameter \beta accounts for any deviations from the axisymmetric case and is used in the calculation of the reduced modulus in equation (10). Currently, the default value is the value for three-sided pyramides \beta=1.034. The value supplied by the user is saved in the settings and can be reset to its default value.

  • Fit buttons for the two fits, see section 5.2 for details of the calculation.

  • Results displays all results in the following order: the residual depth h_{\mathrm{p}}, the power m of the power law function, the parameter \varepsilon, the contact depth h_{\mathrm{c}}, the slope S, the contact area A_{\mathrm{p}}(h_{\mathrm{c}}), the indentation hardness H_{IT}, the contact modulus E_{r}, the indentation modulus E_{IT} and the ranges used for the fitting procedures. The variables are described in detail in section 5.2.

  • Save save parameters and results to given file.

  • Graph display the unloading curve and the fitted curves. Stepwise zooming/unzooming can be performed by selecting a range with the mouse and pressing the Zoom/ Unzoom buttons. The graph is restored to its original size by the Restore button.

5.2 Procedure

The standard calculation consists of three steps

  1. 1.

    The residual depth must be determined as the intersection of the unloading curve and the x-axis. This is implemented by fitting a straight line using a Deming fit with \delta=1, see section A.2. For a brief description of the Deming fit see section A.2

    F=a_{\mathrm{h_{\mathrm{p}}}}h_{\mathrm{p}}+b_{\mathrm{h_{p}}} (2)

    using total least squares. This fit is called the h_{\mathrm{p}} fit. The residual depth is calculated as

    h_{\mathrm{p}}=-b_{h_{\mathrm{p}}}/a_{h_{\mathrm{p}}}. (3)

    The range of the data must be chosen adequately, the range 0.5–15 % F{}_{\mathrm{max}} is often a reasonable value.

  2. 2.

    The main part of the unloading curve is fitted by a power law function

    F=\alpha(h-h_{\mathrm{p}})^{m}. (4)

    This is converted to a total least squares fit in the variables using a Deming fit with \delta=1, see section A.2

    \log F=\log\alpha+m\log(h-h_{\mathrm{p}}). (5)

    The range should not contain the lower part of the unloading range, a range of 40–98 % F{}_{\mathrm{max}} is recommended as a first guess.

  3. 3.

    The auxiliary parameter \varepsilon is calculated from the power m

\pi}\Gamma\left(\frac{1}{2(m-1)}\right)}\right), (6)

    \Gamma is the Gamma-function.
    The contact depth is calculated as

    h_{\mathrm{c}}=h_{\mathrm{max}}-\epsilon\frac{F_{\mathrm{max}}}{S} (7)

    and the slope at the maximum depth as

    S=m\frac{F_{\mathrm{max}}}{h_{\mathrm{max}}-h_{\mathrm{p}}}. (8)
  4. 4.

    The contact depth is used to evaluate the contact area A(h_{\mathrm{c}}). This can be used to find the indentation hardness

    H_{\mathrm{IT}}=\frac{F_{\mathrm{max}}}{A(h_{\mathrm{c}})}. (9)

    and together with the slope to find the contact modulus

    E_{\mathrm{r}}=\sqrt{\pi}\frac{S}{2\beta\sqrt{A(h_{\mathrm{c}})}}. (10)

    For a comparison with Young’s modulus found in literature it is useful to calculate the indentation modulus E_{IT}

\mathrm{i}}}. (11)

    Here \nu is the Poisson’s value of the sample and \nu_{\mathrm{i}} and E_{\mathrm{i}} are the Poisson’s value and the modulus of the indenter.